Acetic Anhydride → HCID 21105567, compound

HRID 2426626Notes

Reaction equation

HRID 2426626 reaction equation
C(O[C:5](=[O:7])[CH3:6])(=O)C.[N+:8]([C:11]1[CH:16]=[CH:15][C:14]([N:17]2[CH2:20][CH:19]([NH2:21])[CH2:18]2)=[CH:13][CH:12]=1)([O-:10])=[O:9]>N1C=CC=CC=1>[N+:8]([C:11]1[CH:12]=[CH:13][C:14]([N:17]2[CH2:18][CH:19]([NH:21][C:5](=[O:7])[CH3:6])[CH2:20]2)=[CH:15][CH:16]=1)([O-:10])=[O:9]

Participants

4

Reactant 2

HCID 7918Acetic AnhydrideHCID 21105370HCID 21105370, compound

Product 1

HCID 21105567HCID 21105567, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

Acetic anhydride (0.6 ml) was added to a solution of 1-(4-nitrophenyl)-azetidin-3-ylamine (0.5 g ) in pyridine (1.2 ml). After one hour, volatile fractions were removed. This resulted in the product with the molecular weight of 235.24 (C11H13N3O3); MS (ESI): 236 (M+H+).

Workup

  1. customvolatile fractions were removed
  2. customThis resulted in the product with the molecular weight of 235.24 (C11H13N3O3)

Sources & evidence

ORD record
ord-095162505de941938c2f09dc8b140224
Source dataset
uspto-grants-2011_06
Patent number
US07968550B2

Reaction notes

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