p-Fluoronitrobenzene → HCID 86594866, compound

HRID 2426628Notes

Reaction equation

HRID 2426628 reaction equation
[NH:1]1[CH2:4][CH:3]([NH:5][C:6](=[O:12])[O:7][C:8]([CH3:11])([CH3:10])[CH3:9])[CH2:2]1.F[C:14]1[CH:19]=[CH:18][C:17]([N+:20]([O-:22])=[O:21])=[CH:16][CH:15]=1>>[N+:20]([C:17]1[CH:18]=[CH:19][C:14]([N:1]2[CH2:4][CH:3]([NH:5][C:6](=[O:12])[O:7][C:8]([CH3:9])([CH3:11])[CH3:10])[CH2:2]2)=[CH:15][CH:16]=1)([O-:22])=[O:21]

Participants

3

Reactant 2

HCID 9590p-FluoronitrobenzeneHCID 15194053-Aminoazetidine, 3-BOC protected

Product 1

HCID 86594866HCID 86594866, compound

Procedure

tert-Butyl azetidin-3-ylcarbamate was reacted with 4-fluoronitrobenzene by method C. This resulted in the product with the molecular weight of 293.33 (C14H19N3O4); MS (ESI): 294 (M+H+).

Workup

  1. customThis resulted in the product with the molecular weight of 293.33 (C14H19N3O4)

Sources & evidence

ORD record
ord-2c964a5e3e4a4d018576cfd959858ba3
Source dataset
uspto-grants-2011_06
Patent number
US07968550B2

Reaction notes

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