HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 21105616, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 21105492 | HCID 21105492 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 21105616 | HCID 21105616 | — |
Reaction Steps
4-Cyclohexyl-N-methyl-N-[4-(4-methylamino-2-oxo-pyrrolidin-1-yl)phenyl]benzamide (101 mg) was mixed with pyridine (20 mg) and acetic anhydride (25 mg) and, after 3 hours, volatile fractions were removed in vacuo. This resulted in the product with the molecular weight of 447.58 (C27H33N3O3); MS (ESI): 448 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07968550B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-d509b1ee84ad412980748f6a80e67301 |
| Source note | uspto-grants-2011_06 |