5-Chloro-2-picolinic acid → HCID 67147784, compound

HRID 2426675Notes

Reaction equation

HRID 2426675 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH2:12][CH2:11][CH:10]([N:13]([CH3:15])[CH3:14])[CH2:9]2)=[CH:4][CH:3]=1.[Cl:16][C:17]1[CH:18]=[CH:19][C:20]([C:23](O)=[O:24])=[N:21][CH:22]=1>>[CH3:14][N:13]([CH3:15])[CH:10]1[CH2:11][CH2:12][N:8]([C:5]2[CH:6]=[CH:7][C:2]([NH:1][C:23]([C:20]3[CH:19]=[CH:18][C:17]([Cl:16])=[CH:22][N:21]=3)=[O:24])=[CH:3][CH:4]=2)[CH2:9]1

Participants

3

Reactant 2

HCID 27628725-Chloro-2-picolinic acidHCID 219165911-(4-aminophenyl)-N,N-dimethylpyrrolidin-3-amine

Product 1

HCID 67147784HCID 67147784, compound

Procedure

[1-(4-Aminophenyl)pyrrolidin-3-yl]dimethylamine was reacted with 5-chloropyridine-2-carboxylic acid by method E. This resulted in the product with the molecular weight of 344.85 (C18H21CIN4O); MS (ESI): 345 (M+H+).

Workup

  1. customThis resulted in the product with the molecular weight of 344.85 (C18H21CIN4O)

Sources & evidence

ORD record
ord-f9d138fd658a46beafee4d29a4bf1632
Source dataset
uspto-grants-2011_06
Patent number
US07968550B2

Reaction notes

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