HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2426746Generated: October 26, 2026
Ethanol → 6-Methoxy-2',6'-dimethylbiphenyl-3-carbaldehyde
https://huagongshe.com/reaction/2426746
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 2-Bromo-m-xylene | HCID 68471 | — |
| Reactant | 5-Formyl-2-methoxyphenylboronic acid | HCID 2734367 | — |
| Catalyst | HCID 178418397 | HCID 178418397 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | 6-Methoxy-2',6'-dimethylbiphenyl-3-carbaldehyde | HCID 57787305 | — |
Reaction Steps
In an atmosphere of nitrogen, tetrakis(triphenylphosphine)palladium was added to a mixture of 2-bromo-1,3-dimethylbenzene, (5-formyl-2-methoxyphenyl)boronic acid, a 1 M sodium carbonate aqueous solution, ethanol and dimethoxyethane, followed by stirring at 80° C. for 25 hours to obtain 6-methoxy-2′,6′-dimethylbiphenyl-3-carbaldehyde.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07968552B2 |
|---|
| Source dataset | uspto-grants-2011_06 |
|---|
| ORD ID | ord-10e8261531c149c8bb14835d0b23a899 |
|---|
| Source note | uspto-grants-2011_06 |
|---|
