HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2426776Generated: November 2, 2026
Potassium Phosphate, Tribasic → HCID 57787402, compound
https://huagongshe.com/reaction/2426776
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Phosphate, Tribasic | HCID 62657 | — |
| Reactant | 2-Dicyclohexylphosphino-2',6'-dimethoxybiphenyl | HCID 11269872 | — |
| Reactant | B-[4-[[(1,1-Dimethylethyl)dimethylsilyl]oxy]-2-methylphenyl]boronic acid | HCID 21107088 | — |
| Reactant | HCID 57787358 | HCID 57787358 | — |
| Catalyst | palladium(II) acetate | HCID 167845 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 57787402 | HCID 57787402 | — |
Reaction Steps
In an atmosphere of nitrogen, a mixture of (4-{[tert-butyl(dimethyl)silyl]oxy}-2-methylphenyl)boronic acid, 6-[(3-bromo-2-methylbenzyl)oxy]nicotinaldehyde, palladium acetate, dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine, tripotassium phosphate, toluene and water was stirred with heating at 60° C. for 2 days to obtain 6-[(4′-{[tert-butyl(dimethyl)silyl]oxy}-2,2′-dimethylbiphenyl-3-yl)methoxy]nicotinaldehyde.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07968552B2 |
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| Source dataset | uspto-grants-2011_06 |
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| ORD ID | ord-c1670cb36bc442fca6ee72adedc94057 |
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| Source note | uspto-grants-2011_06 |
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