HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzoic Acid → N-[3-(methylsulfanyl)phenyl]-4-nitrobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzoic Acid | HCID 6108 | — |
| Reactant | Benzenamine, 3-(methylthio)- | HCID 15693 | — |
| Product | N-[3-(methylsulfanyl)phenyl]-4-nitrobenzamide | HCID 873432 | 85.3% |
Reaction Steps
Using 3-methylthioaniline (1.40 ml, 11.0 mmol) and 4-nitrobenzoic acid (1.67 g, 10.0 mmol), the procedure of Reference Example 16 was repeated to obtain 2.46 g (85.2%) of the title compound in the form of yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05728835 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-bac4f35022814f6eaa0f9cad74b4ef8c |
| Source note | uspto-grants-1998_03 |