HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 86632552, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 57780058 | HCID 57780058 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86632552 | HCID 86632552 | 98.4% |
Reaction Steps
In 10 ml of N,N-dimethylformamide was dissolved 0.65 g of 1-(2,6-dichlorophenyl)-1H-pyrrole-2-carbaldehyde, and then 0.53 g of N-bromosuccinimide was added thereto. The mixture was stirred at room temperature for 1 hour. Water was poured into the reaction mixture, a deposited precipitate was collected by filtration to obtain 0.85 g of 4-bromo-1-(2,6-dichlorophenyl)-1H-pyrrole-2-carbaldehyde of the formula:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07968573B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-b207cbc65d9a4a22b96f6fcc402ea4e2 |
| Source note | uspto-grants-2011_06 |