反应详情

A solution of 2-bromo-1-[3-(trifluoromethyl)phenyl]ethanone (1 g) in acetonitrile (2.5 mL) and water (10 mL) is treated under microwave irradiation (125° C., 50 min) The same experiment is repeated five times. All the vials are collected, extracted with DCM, dried over magnesium sulfate and concentrated under vacuum to give the desired compound.

1. customAll the vials are collected
2. extractionextracted with DCM
3. dry with materialdried over magnesium sulfate
4. concentrationconcentrated under vacuum