HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl xanthate → HCID 178423568, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl xanthate | HCID 8823 | — |
| Reactant | Potassium | HCID 5462222 | — |
| Reactant | 2-Bromo-5-methylaniline | HCID 6422065 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178423568 | HCID 178423568 | — |
Reaction Steps
The title compound was prepared using the method of example 239, starting with 2-bromo-5-methyl-phenylamine (244) (4.48 g, 24.0 mmol), O-ethylxanthic acid, potassium salt (Lancaster, 8.70 g, 54 mmol) in DMF (35 mL). The mercaptobenzothiazole 245 was obtained as an pale brown solid (2.31 g, 53%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07968567B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-8ff22b74d5244a358671dda2ca1f824e |
| Source note | uspto-grants-2011_06 |