HCID 10609383, compound → HCID 10535968, compound

Participants

Reaction Steps

A mixture of (4-methyl-2-nitrophenyl)phenylamine (1.41 g, 6.18 mmol) and 10% Pd/C (140 mg) in EtOAc (30 mL) was degassed with a stream of nitrogen and stirred at RT under a hydrogen atmosphere for 5 h. The suspension was then filtered through a PTFE frit and the filtrate was concentrated in vacuo affording 4-Methyl-N1-phenylbenzene-1,2-diamine as an off-white solid (1.18 g, 96%). LCMS: RT 3.08 min [M+H]+ 199.1.

Provenance & Evidence