HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ceric ammonium nitrate → 2-Hydroxy-2-methyl-n-propyl-4-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dienyl)butanamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ceric ammonium nitrate | HCID 180504 | — |
| Edukt | 6-hydroxy-2,5,7,8-tetramethyl-N-propylchroman-2-carboxamide | HCID 67262969 | — |
| Produkt | 2-Hydroxy-2-methyl-n-propyl-4-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dienyl)butanamide | HCID 42598874 | — |
Reaktionsschritte
Oxidation as described in protocol B, using 90.6 mg (0.311 mmol) of 6-hydroxy-2,5,7,8-tetramethyl-N-propylchroman-2-carboxamide and 374.9 mg CAN (0.684 mmol) yielded 2-hydroxy-2-methyl-N-propyl-4-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dienyl)butanamide as a yellow powder.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07968746B2 |
| Quelldatensatz | uspto-grants-2011_06 |
| ORD ID | ord-304857be3eef452c9bfdc238b909cbab |
| Quellennotiz | uspto-grants-2011_06 |