HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tyramine → HCID 67263027, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tyramine | HCID 5610 | — |
| Reactant | Trolox | HCID 40634 | — |
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Product | HCID 67263027 | HCID 67263027 | 72.8% |
Reaction Steps
Following the amide coupling procedure described in protocol A, 500 mg 6-hydroxy-2,5,7,8-tetramethylchroman-2-carboxylic acid (2.0 mmol), 356 mg CDI (2.2 mmol) and 548 mg tyramine (4.0 mmol) produced 537.8 mg of 6-hydroxy-N-(4-hydroxyphenethyl)-2,5,7,8-tetramethylchroman-2-carboxamide as a brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07968746B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-209ad26bb1a9448d88d2484ecd6ea44a |
| Source note | uspto-grants-2011_06 |