HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxyaniline → N-(3-Methoxy-phenyl)-2-nitro-benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxyaniline | HCID 10824 | — |
| Reactant | 2-Nitrobenzoic acid | HCID 11087 | — |
| Product | N-(3-Methoxy-phenyl)-2-nitro-benzamide | HCID 542853 | 85% |
Reaction Steps
Using m-anisidine (2.03 g, 16.5 mmol) and 2-nitrobenzoic acid (2.51 g, 15.0 mmol), the procedure of Reference Example 16 was repeated to obtain 3.47 g (84.9%) of the title compound in the form of light yellow needle crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05728835 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-dfd5a32f672c46c19f0d787eab887512 |
| Source note | uspto-grants-1998_03 |