HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzoic Acid → 4'-Fluoro-4-nitrobenzanilide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzoic Acid | HCID 6108 | — |
| Reactant | 4-Fluoroaniline | HCID 9731 | — |
| Product | 4'-Fluoro-4-nitrobenzanilide | HCID 306568 | 65.8% |
Reaction Steps
Using 4-fluoroaniline (1.0 ml, 9.93 mmol) and 4-nitrobenzoic acid (1.58 g, 9.36 mmol), the procedure of Reference Example 16 was repeated to obtain 1.60 g (65.8%) of the title compound in the form of light yellow needle crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05728835 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-6dae5ade71d64ef5bed47b84c6e2b2bc |
| Source note | uspto-grants-1998_03 |