HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Ethoxybenzoic acid → HCID 52917316, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Ethoxybenzoic acid | HCID 67252 | — |
| Reactant | HCID 60916944 | HCID 60916944 | — |
| Product | HCID 52917316 | HCID 52917316 | — |
Reaction Steps
The title compound was prepared according to the procedure used for Example 15 utilizing 2-(4-methoxy-pyrimidin-2-yl)-octahydro-pyrrolo[3,4-c]pyrrole and 2-ethoxybenzoic acid. MS (ESI) mass calcd. for C20H24N4O3, 368.44; m/z found, 369.3 [M+H]+. 1H NMR (CDCl3): 8.07 (d, J=5.7 Hz, 1H), 7.37-7.28 (m, 2H), 6.99 (t, J=7.4 Hz, 1H), 6.91 (d, J=8.3 Hz, 1H), 6.02 (d, J=5.7 Hz, 1H), 4.07 (q, J=7.0 Hz, 2H), 4.01-3.85 (m, 5H), 3.84-3.70 (m, 2H), 3.65-3.45 (m, 3H), 3.34-3.22 (m, 1H), 3.16-2.92 (m, 2H), 1.35 (t, J=6.8 Hz, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08653263B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-548709e3140d406fb4f2881f5eade2a4 |
| Source note | uspto-grants-2014_02 |