o-Phenylbenzoic acid → HCID 67116825, compound

HRID 243977Notes

Reaction equation

HRID 243977 reaction equation
[CH2:1]1[CH:5]2[CH2:6][NH:7][CH2:8][CH:4]2[CH2:3][N:2]1[C:9]1[CH:18]=[N:17][C:16]2[C:11](=[CH:12][CH:13]=[CH:14][CH:15]=2)[N:10]=1.[C:19]1([C:28]2[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=2)[C:20]([C:25](O)=[O:26])=[CH:21][CH:22]=[CH:23][CH:24]=1>>[C:19]1([C:28]2[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=2)[CH:24]=[CH:23][CH:22]=[CH:21][C:20]=1[C:25]([N:7]1[CH2:6][CH:5]2[CH2:1][N:2]([C:9]3[CH:18]=[N:17][C:16]4[C:11](=[CH:12][CH:13]=[CH:14][CH:15]=4)[N:10]=3)[CH2:3][CH:4]2[CH2:8]1)=[O:26]

Participants

3

Reactant 2

HCID 70357o-Phenylbenzoic acidHCID 610372812-(Hexahydro-pyrrolo[3,4-c]pyrrol-2-yl)-quinoxaline

Product 1

HCID 67116825HCID 67116825, compound

Procedure

The title compound was prepared in a manner analogous to Example 15 utilizing Intermediate 35 and biphenyl-2-carboxylic acid. MS (ESI) mass calcd. for C27H24N4O, 420.52; m/z found, 421.3 [M+H]+.

Sources & evidence

ORD record
ord-c877febfaba649e1b3699cca4ac99b84
Source dataset
uspto-grants-2014_02
Patent number
US08653263B2

Reaction notes

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