2-(4-Methylphenyl)benzoic acid → HCID 67116791, compound

HRID 243997Notes

Reaction equation

HRID 243997 reaction equation
[CH2:1]1[CH:5]2[CH2:6][NH:7][CH2:8][CH:4]2[CH2:3][N:2]1[C:9]1[CH:18]=[N:17][C:16]2[C:11](=[CH:12][CH:13]=[CH:14][CH:15]=2)[N:10]=1.[CH3:19][C:20]1[CH:25]=[CH:24][C:23]([C:26]2[C:27]([C:32](O)=[O:33])=[CH:28][CH:29]=[CH:30][CH:31]=2)=[CH:22][CH:21]=1>>[CH3:19][C:20]1[CH:21]=[CH:22][C:23]([C:26]2[CH:31]=[CH:30][CH:29]=[CH:28][C:27]=2[C:32]([N:7]2[CH2:8][CH:4]3[CH:5]([CH2:1][N:2]([C:9]4[CH:18]=[N:17][C:16]5[C:11](=[CH:12][CH:13]=[CH:14][CH:15]=5)[N:10]=4)[CH2:3]3)[CH2:6]2)=[O:33])=[CH:24][CH:25]=1

Participants

3

Reactant 2

HCID 815682-(4-Methylphenyl)benzoic acidHCID 610372812-(Hexahydro-pyrrolo[3,4-c]pyrrol-2-yl)-quinoxaline

Product 1

HCID 67116791HCID 67116791, compound

Procedure

The title compound was prepared in a manner analogous to Example 15 utilizing Intermediate 35 and 4′-methyl-biphenyl-2-carboxylic acid. MS (ESI): mass calculated for C28H26N4O, 434.55; m/z found 435.3 [M+H]+.

Sources & evidence

ORD record
ord-54f5bdec9a0648909539fcaccb77a21f
Source dataset
uspto-grants-2014_02
Patent number
US08653263B2

Reaction notes

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