HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Difluorobenzoic acid → HCID 67116314, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Difluorobenzoic acid | HCID 9796 | — |
| Reactant | 2-(4,6-Dimethylpyrimidin-2-yl)octahydropyrrolo[3,4-c]pyrrole | HCID 66210875 | — |
| Product | HCID 67116314 | HCID 67116314 | — |
Reaction Steps
The title compound was prepared in a manner analogous to Example 15, utilizing Intermediate 23 and 2,6-difluorobenzoic acid. MS (ESI): mass calculated for C19H20F2N4O, 358.16; m/z found 359.2 [M+H]+. 1H NMR (400 MHz, CDCl3): 7.34 (tt, J=8.4, 6.4, 1H), 6.93 (s, 2H), 6.30 (s, 1H), 4.12-3.76 (m, 3H), 3.75-3.45 (m, 4H), 3.36-2.88 (m, 3H), 2.30 (s, 6H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08653263B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-00a1679cf3c3474c88d4e5509383388a |
| Source note | uspto-grants-2014_02 |