HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Dichloroethane → HCID 58579585, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Dichloroethane | HCID 6365 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Benzoic acid, 4-amino-, 1,1-dimethylethyl ester | HCID 233272 | — |
| Reactant | Benzene-1,2-disulfonyl dichloride | HCID 246432 | — |
| Product | HCID 58579585 | HCID 58579585 | — |
Reaction Steps
Following the General Procedure (Scheme 1), tert-butyl 4-aminobenzoate, 1, (1.0 g, 5.17 mmol), triethylamine (1.8 mL, 12.9 mmol), dichloroethane (75 mL), benzene-1,2-disulfonyl dichloride (1.7 g, 2.88 mmol) and dichloroethane afforded tert-butyl-4-(1,1,3,3-tetraoxidobenzo[d][1,3,2]dithiazol-2-yl)benzoate, 5, (0.39 g, 38%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08658650B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-f12cf88890d04f91bd83b79ee61d5714 |
| Source note | uspto-grants-2014_02 |