Sodium borohydride → HCID 51347903, compound

Participants

Reaction Steps

To a solution of 7 (17 mg, 0.03 mmol) (Example 1) in MeOH (3 mL) was added NaBH4 (20 mg, 0.5 mmol). The mixture was stirred at room temperature for 3 hrs before it was concentrated to dryness. The residue was purified on a prep TLC plate eluting with 10% ammonia /MeOH (2 M) in CH2Cl2 to yield a yellow solid 31 (10 mg, 59%). LCMS M+1=578.3 retention time=1.70 min.

Provenance & Evidence