HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzoyl chloride → N-(1,3-benzodioxol-5-yl)-4-nitrobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzoyl chloride | HCID 8502 | — |
| Reactant | 1,3-Benzodioxol-5-amine | HCID 84310 | — |
| Product | N-(1,3-benzodioxol-5-yl)-4-nitrobenzamide | HCID 674221 | 87.2% |
Reaction Steps
Using 3,4-methylenedioxyaniline (1.44 g, 10.5 mmol) and 4-nitrobenzoyl chloride (1.86 g, 10.0 mmol), the procedure of Reference Example 11 was repeated to obtain 2.49 g (87.2%) of the title compound in the form of yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05728835 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-b04fe9c2f1da4526a30f3f2067ac49b1 |
| Source note | uspto-grants-1998_03 |