HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl(5,6-diethyl-2-methyl-indan-2-yl)-amine → 5,6-Diethyl-2-methyl-indan-2-ylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl(5,6-diethyl-2-methyl-indan-2-yl)-amine | HCID 22499185 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 5,6-Diethyl-2-methyl-indan-2-ylamine | HCID 22499232 | — |
Reaction Steps
A solution of benzyl-(5,6-diethyl-2-methyl-indan-2-yl)-amine (0.48 g) in methanol (10 ml) is stirred under an atmosphere of hydrogen in the presence of 10% Pd/C at room temperature for 18 hours. The mixture is filtered through celite and the filtrate is concentrated in vacuo to give the title compound. ES+ MS m/e 204 (MH+)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08658673B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-da13bab96e854ff5ac40be3bc6fd1382 |
| Source note | uspto-grants-2014_02 |