Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | Lithium perchlorate | HCID 23665649 | — |
| Reactant | HCID 89510183 | HCID 89510183 | — |
| Product | HCID 89510172 | HCID 89510172 | — |
Reaction Steps
The title compound is prepared by essentially following the procedure as described in Preparation 41 using rel-tert-butyl-[[(1R,4S,5R)-5-methyl-6-oxabicyclo[3.1.0]hexan-4-yl]oxy]-diphenyl-silane (enantiomeric mixture), except that the reaction is heated to 90° C. for 48 h and the addition of lithium perchlorate and the second addition of sodium azide are omitted.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08658693B2 |
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| Source dataset | uspto-grants-2014_02 |
|---|
| ORD ID | ord-f0dfeb3cdf7348c7bb96aaa8a6e4db54 |
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| Source note | uspto-grants-2014_02 |
|---|
