HCID 66932383, compound → HCID 178436625, compound

HRID 245096Notes

Reaction equation

HRID 245096 reaction equation
N[C:2]1C(C)=CC(C#N)=C[C:3]=1CC.Cl[C:14]1[CH:15]=[C:16]([CH:21]=[C:22]([CH3:29])[C:23]=1[NH:24][S:25]([CH3:28])(=[O:27])=[O:26])[C:17]([NH:19][OH:20])=[NH:18]>>[CH2:2]([C:14]1[CH:15]=[C:16]([CH:21]=[C:22]([CH3:29])[C:23]=1[NH:24][S:25]([CH3:28])(=[O:27])=[O:26])[C:17]([NH:19][OH:20])=[NH:18])[CH3:3]

Participants

3

Reactant 2

HCID 66932383HCID 66932383, compoundHCID 178426664HCID 178426664, compound

Product 1

HCID 178436625HCID 178436625, compound

Procedure

The title compound is then prepared from the above 4-amino-3-ethyl-5-methyl-benzonitrile in analogy to 3-chloro-N-hydroxy-4-methanesulfonylamino-5-methyl-benzamidine; LC-MS**: tR=0.26 min, [M+1]+=272.32.

Sources & evidence

ORD record
ord-36061704a55f4bb19ddae774b57f521c
Source dataset
uspto-grants-2014_02
Patent number
US08658675B2

Reaction notes

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