HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-(1,3-Dioxolan-2-yl)-2,6-dimethoxyphenyl)boronic acid → N-(2,6-dichlorobenzoyl)-4-[4-(1,3-dioxolan-2-yl)-2,6-dimethoxyphenyl]-L-phenylalanine methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-(1,3-Dioxolan-2-yl)-2,6-dimethoxyphenyl)boronic acid | HCID 22571993 | — |
| Reactant | HCID 22970630 | HCID 22970630 | — |
| Product | N-(2,6-dichlorobenzoyl)-4-[4-(1,3-dioxolan-2-yl)-2,6-dimethoxyphenyl]-L-phenylalanine methyl ester | HCID 54069836 | — |
Reaction Steps
4-(1,3-Dioxolan-2-yl)-2,6-dimethoxybenzeneboronic acid was reacted with N-(2,6-dichlorobenzoyl)-O-(trifluoromethanesulfonyl)-L-tyrosine methyl ester in a similar manner as described in Example 7-2) to give N-(2,6-dichlorobenzoyl)-4-[4-(1,3-dioxolan-2-yl)-2,6-dimethoxyphenyl]-L-phenylalanine methyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06855843B2 |
| Source dataset | uspto-grants-2005_02 |
| ORD ID | ord-e857d116ff8a4c98850eaedfb08542f6 |
| Source note | uspto-grants-2005_02 |