HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl ester phosphorous acid → 1,2-Dihydroxypropane Dodecyl Sulfide Phosphite
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl ester phosphorous acid | HCID 94853 | — |
| Reactant | 1,2-Dihydroxypropane dodecyl sulfide | HCID 86739775 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1,2-Dihydroxypropane Dodecyl Sulfide Phosphite | HCID 86741852 | — |
Reaction Steps
Approximately 100 g of the above 1,2-dihydroxypropane dodecyl sulfide was reacted with 15 g dimethyl hydrogen phosphite as generally described in Example 1 until methanol evolution ceased. The product was vacuum-distilled to remove volatile materials.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04704218 |
| Source dataset | uspto-grants-1987_11 |
| ORD ID | ord-04645eb165d84049b314e94a88e1b4eb |
| Source note | uspto-grants-1987_11 |