HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium → HCID 86741860, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 20161189 | HCID 20161189 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86741860 | HCID 86741860 | 93% |
Reaction Steps
1,2-Dihydro-N-hydroxy-6,7-dimethoxy-naphthalene-3-carboxamide (2.5 g) was added to a stirred solution of sodium metal (0.227 g) in methanol (55 ml). After 15 min. the solution was evaporated to dryness and the residue crystallised from methanol:ether to give 2.5 g of the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04705782 |
| Source dataset | uspto-grants-1987_11 |
| ORD ID | ord-d2db3ea503d84595b2d11978882ca5dd |
| Source note | uspto-grants-1987_11 |