HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Dimethoxyethyl(dimethyl)amine → HCID 88646181, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Dimethoxyethyl(dimethyl)amine | HCID 87835 | — |
| Reactant | HCID 11805035 | HCID 11805035 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Product | HCID 88646181 | HCID 88646181 | — |
Reaction Steps
A mixture of 4.7 g of N(dimethylaminomethylene)-glycine-ethyl ester (W. Kantlehner et al., Liebigs Ann. Chem. 1980, 344), 8 g of dimethylacetamide-dimethylacetal and 0.4 g of potassium tert-butylate, analogously to 1b), is heated for 8 hours with distilling off of the resulting alcohols. The residue is fractionated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04705856 |
| Source dataset | uspto-grants-1987_11 |
| ORD ID | ord-df94d5bc02324e979c2abcf1fdc43743 |
| Source note | uspto-grants-1987_11 |