Methyl iodide → Methyl N-(2,6-dichlorobenzyl)dithiocarbamate

HRID 247409Notes

Reaction equation

[Cl:1][C:2]1[CH:9]=[CH:8][CH:7]=[C:6]([Cl:10])[C:3]=1[CH2:4][NH2:5].[C:11](=[S:13])=[S:12].I[CH3:15]>>[Cl:1][C:2]1[CH:9]=[CH:8][CH:7]=[C:6]([Cl:10])[C:3]=1[CH2:4][NH:5][C:11](=[S:13])[S:12][CH3:15]

Participants

Reactant 3

HCID 6328Methyl iodide

HCID 6348Carbon Disulfide

HCID 485432Benzenemethanamine, 2,6-dichloro-

Product 1

HCID 14049926Methyl N-(2,6-dichlorobenzyl)dithiocarbamateYield 32%

Procedure

2,6-Dichlorobenzylamine (0.020 mol) was reacted with carbon disulfide (0.020 mol) and iodomethane (0.019 mol) substantially as described in Example 1B above to obtain 1.5 g (32%) white crystals: mp 47°.

Sources & evidence

ORD record: ord-f83dc7a65cf74d4d9c02b7a86857070d
Source dataset: uspto-grants-1987_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04707488

Reaction notes

Loading…