Sodium Azide → HCID 178527992, compound

HRID 247412Notes

Reaction equation

HRID 247412 reaction equation
[C:1]1([CH2:7][CH2:8][CH2:9][NH:10][C:11](=[S:14])SC)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[N-:15]=[N+:16]=[N-:17].[Na+]>>[C:1]1([CH2:7][CH2:8][CH2:9][N:10]2[C:11]([SH:14])=[N:17][N:16]=[N:15]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 33557Sodium AzideHCID 14581310Methyl (3-phenylpropyl)carbamodithioate

Product 1

HCID 178527992HCID 178527992, compoundYield 21%

Procedure

Methyl N-(3-phenylpropyl)dithiocarbamate (0.044 mol) and sodium azide (0.062 mol) were reacted substantially as described in Example 1C above to obtain 2.0 g (21%) colorless crystals: mp 75°-76° (pet. ether).

Sources & evidence

ORD record
ord-f79caaa7dd804a94bb5294c811359c02
Source dataset
uspto-grants-1987_11
Patent number
US04707488

Reaction notes

Loading…