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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 247426Generated: October 31, 2026

4-Toluenesulfonyl chloride → 3-(3,5-Dichlorophenyl)propylazide

https://huagongshe.com/reaction/247426

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Toluenesulfonyl chlorideHCID 7397—
ReactantSodium AzideHCID 33557—
Reactant3,5-DichlorobenzenepropanolHCID 14581315—
Product3-(3,5-Dichlorophenyl)propylazideHCID 1458131698%

Reaction Steps

3-(3,5-Dichlorophenyl)propanol (0.052 mol), tosyl chloride (0.104 mol) and sodium azide (0.104 mol) were reacted substantially as described in Example 7E to obtain 11.7 g (98%) of an oily product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04707488
Source datasetuspto-grants-1987_11
ORD IDord-59b841bb6a87493696afd72622dd73ea
Source noteuspto-grants-1987_11