Sodium Azide → HCID 178490139, compound

HRID 247429Notes

Reaction equation

HRID 247429 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][CH2:11][N:12]=[C:13]=[S:14])=[CH:5][CH:4]=1.[N-:15]=[N+:16]=[N-:17].[Na+]>>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][CH2:11][N:12]2[C:13]([SH:14])=[N:17][N:16]=[N:15]2)=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 33557Sodium AzideHCID 14581319HCID 14581319, compound

Product 1

HCID 178490139HCID 178490139, compoundYield 55.1%

Procedure

3-(4-Methoxyphenyl)propylisothiocyanate (0.0174 mol) and sodium azide (0.0261 mol) were reacted substantially as described in Example 7H to give 2.4 g (55%) of an orange oil.

Sources & evidence

ORD record
ord-59a75041ec274d1f8d6ddf824c560684
Source dataset
uspto-grants-1987_11
Patent number
US04707488

Reaction notes

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