참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Azobisisobutyronitrile | HCID 6547 | — |
| 반응물 | Acrylic Acid | HCID 6581 | — |
| 반응물 | Lauryl Methacrylate | HCID 8906 | — |
| 반응물 | 2,2'-Azobis(2,4-dimethylvaleronitrile) | HCID 91537 | — |
| 생성물 | Laurylmethacrylate Acrylic Acid | HCID 86741893 | 33% |
반응 단계
To 795.4 g of laurylmethacrylate is added 4.64 g of glacial acrylic acid and 800 g of liquid hydrocarbon sold commercially as Isopar® M by Exxon. Then 0.8 g of 2,2'-azobis(2,4-dimethylvaleronitrile) which is sold commercially as Vazo® 52 by E. I. duPont de Nemours Corporation is added. The solution is agitated, purged with nitrogen for 1 hour and then heated to 50° C. After 12 hours of heating, the temperature of the thickened solution is increased to 60° C. and held there for 2 hours. It is then cooled and mixed with another 800 g of the aforementioned liquid hydrocarbon to give a 33 percent polymer solution.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04708997 |
|---|
| 출처 데이터셋 | uspto-grants-1987_11 |
|---|
| ORD ID | ord-3123c02ade5f478e8cb06b0adcc5a922 |
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| 출처 메모 | uspto-grants-1987_11 |
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