1-Propanol, 3-amino-2,2-dimethyl- → HCID 178438303, compound

HRID 247602Notes

Reaction equation

HRID 247602 reaction equation
[CH2:1]([C:4]12[CH2:10][CH:7]([CH:8]=[CH:9]1)[CH:6]1[C:11]([O:13][C:14](=[O:15])[CH:5]21)=[O:12])[CH:2]=[CH2:3].[CH3:16][C:17]([CH2:21][OH:22])([CH2:19][NH2:20])[CH3:18]>>[CH3:16][C:17]([CH3:18])([CH2:21][OH:22])[CH2:19][N:20]=[C:14]([CH:5]1[CH:6]([C:11]([OH:13])=[O:12])[CH:7]2[CH2:10][C:4]1([CH2:1][CH:2]=[CH2:3])[CH:9]=[CH:8]2)[OH:15]

Participants

3

Reactant 2

HCID 1173261-Propanol, 3-amino-2,2-dimethyl-HCID 54206110Allylbicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic anhydride

Product 1

HCID 178438303HCID 178438303, compound

Procedure

204 g of allylbicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid anhydride are reacted with 103 g of neopentanolamine for 4 hours at 120° C., and the product is isolated by distillation. 268 g (92.7% of theory) of a yellow oil with a refractive index n25D of 1.5190 and a viscosity of 6.21 Pa.s are obtained at a temperature in the range from 169° to 172° C. at 2.53 Pa.

Workup

  1. customthe product is isolated by distillation
  2. custom268 g (92.7% of theory) of a yellow oil with a refractive index n25D of 1.5190 and a viscosity of 6.21 Pa.s are obtained at a temperature in the range from 169° to 172° C. at 2.53 Pa

Sources & evidence

ORD record
ord-3259c55295c046d9adb4c989b102b962
Source dataset
uspto-grants-1987_11
Patent number
US04709047

Reaction notes

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