Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diglycolamine | HCID 13578 | — |
| Reactant | Allylbicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic anhydride | HCID 54206110 | — |
| Product | HCID 178438305 | HCID 178438305 | 78.4% |
Reaction Steps
120 g of allylbicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid anhydride are reacted with 67.9 g of diglycolamine at 140° C., the reaction mixture is heated to 200° C. and the pressure is lowered to 10.6 Pa, affording 142.6 g of a yellow oil with a viscosity of 1.55 Pa.s at 25° C. and an n25D of 1.5230.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04709047 |
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| Source dataset | uspto-grants-1987_11 |
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| ORD ID | ord-e4096e9e61154b6080e34de61b9e121d |
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| Source note | uspto-grants-1987_11 |
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