HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → N-(2-cycloheptenyl)morpholine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-Bromocyclohept-1-ene | HCID 12453881 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | N-(2-cycloheptenyl)morpholine | HCID 13474806 | 50.2% |
Reaction Steps
A mixture of 3-bromocycloheptene (1.75 g, 10 mmoles), triethylamine (1.01 g, 10 mmoles), morpholine (0.87 g, 10 mmoles) and chloroform (10 ml) was heated under reflux for 3 hours. After completion of the refluxing, the reaction mixture was after-treated as usual and purified by chromatography to obtain 0.91 g of N-(2-cycloheptenyl)morpholine [Compound (3)].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04709052 |
| Source dataset | uspto-grants-1987_11 |
| ORD ID | ord-3cf232795ff34acfaaa551c7010920ce |
| Source note | uspto-grants-1987_11 |