HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N-(4-Nitrophenyl)propionamide → N-(4-Aminophenyl)propanamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N-(4-Nitrophenyl)propionamide | HCID 3627923 | — |
| Edukt | HCID 178418361 | HCID 178418361 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | N-(4-Aminophenyl)propanamide | HCID 314342 | — |
Reaktionsschritte
250 mg (2 mmol) of N-propionyl-4-nitroaniline are dissolved in 200 ml of methanol and combined with 0.6 g of 10% palladium/charcoal. The product is hydrogenated in a hydrogen atmosphere at 2 bar for 30 minutes. Then the catalyst is filtered off and the solvent is eliminated in vacuo.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06855710B2 |
| Quelldatensatz | uspto-grants-2005_02 |
| ORD ID | ord-3b91ba32e4944bce809d7a26b6f46926 |
| Quellennotiz | uspto-grants-2005_02 |