HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 3-Phenoxybenzyl alcohol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Benzenemethanol, 3-phenoxy-, 1-acetate | HCID 170904 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-Phenoxybenzyl alcohol | HCID 26295 | 95% |
Reaction Steps
2.42 g. (0.01 mole) of 3-phenoxybenzyl acetate, 5 cm3. of methanol and 5 cm3. of 2N sodium hydroxide solution are refluxed for three hours. Then the methanol is distilled off and the organic phase is dissolved in 30 cm3. of methylene chloride, washed with 10 cm3. of 1N hydrochloric acid solution and 10 cm3. of water. 1.90 g. of 3-phenoxybenzyl alcohol are obtained. nD20 : 1.593, yield 95%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04709081 |
| Source dataset | uspto-grants-1987_11 |
| ORD ID | ord-1a6f3bb1de714fc18ae39f93cc964184 |
| Source note | uspto-grants-1987_11 |