HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Hydroxy-2-naphthoic acid → 1,1,1-Trifluorooctan-2-YL 6-hydroxynaphthalene-2-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Hydroxy-2-naphthoic acid | HCID 85557 | — |
| Reactant | 2-Octanol, 1,1,1-trifluoro- | HCID 97804 | — |
| Catalyst | Sulfuric Acid | HCID 1118 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 1,1,1-Trifluorooctan-2-YL 6-hydroxynaphthalene-2-carboxylate | HCID 15724811 | — |
Reaction Steps
To a solution of 2-hydroxy-6-carboxynaphthalene (1 g) and optically active 1,1,1-trifluoro-2-octanol (1.1 g) in methylene chloride (50 ml) was added a few drops of conc. sulfuric acid and the mixture was refluxed under stirring for about two days.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05207947 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-43d063be546145bd9ec5526f7bbccb38 |
| Source note | uspto-grants-1993_05 |