HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Decanol → 2-n-Decyloxycarbonylnaphthalene-6-carboxylic acid chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Decanol | HCID 8174 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-Dimethylaminopyridine | HCID 21885 | — |
| Reactant | 2,6-Naphthalenedicarbonyl dichloride | HCID 3485596 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-n-Decyloxycarbonylnaphthalene-6-carboxylic acid chloride | HCID 54316020 | 56.3% |
Reaction Steps
After a solution of n-decyl alcohol (0.5 g), naphthalene-2,6-dicarboxylic acid dichloride (0.6 g), and triethylamine (0.27 g) and a very small amount of dimethylaminopyridine in methylene chloride (50 ml) was stirred at room temperature overnight, the solution was distilled to remove the solvent, until the titled compound (about 0.5 g) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05207947 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-75e52ba2a4e54b1da4dfeb4197a82b67 |
| Source note | uspto-grants-1993_05 |