HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 19091417, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1-benzyl-N-methylpiperidin-4-amine | HCID 4136128 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19091417 | HCID 19091417 | — |
Reaction Steps
0.2 mole of acetyl chloride is slowly added to a solution containing 0.2 mole of N-[1-(benzyl)-4-piperidyl]-N-methylamine, 0.2 mole of triethylamine and 500 cm3 of methylene chloride. The mixture is left in contact for 2 hours, evaporated, taken up in ether and then washed with water. After evaporation, an oil which corresponds to the expected compound is obtained:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05208243 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-a477921d9c324c70a58a84057190fc6b |
| Source note | uspto-grants-1993_05 |