huagongshe.com
HRID247885

反应详情

EQUATION

反应方程式

HRID 247885 的结构方程式

REACTANTS

反应物

2
结构：CN1CC(=O)NC1=O
HCID69217

1-Methylhydantoin

C4H6N2O2

结构：CC(C)c1cc(C=O)cc(C(C)C)c1O
HCID82712

4-Hydroxy-3,5-bis(isopropyl)benzaldehyde

C13H18O2

PRODUCTS

生成物

1
结构：CC(C)c1cc(C=C2C(=O)NC(=O)N2C)cc(C(C)C)c1O
HCID54284051

未命名化合物

收率 11%

PROCEDURE

实验过程

Prepared according to the procedure described in Example 92 using 3,5-diisopropyl-4-hydroxybenzaldehyde (2.7 g, 13 mmoles) and 1-methyl hydantoin (1.4 g, 12 mmoles). Recrystallization from acetonitrile gave the pure product (0.4 g), mp 197°-208° C.

WORKUP

后处理

  1. customPrepared
  2. customRecrystallization from acetonitrile