化工社化工社 化学情報印刷レポート · 研究参考用
Methanol → 3-(Tetradecyloxy)benzoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | Methyl 3-(tetradecyloxy)benzoate | HCID 5152765 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 3-(Tetradecyloxy)benzoic acid | HCID 3262311 | 93.1% |
反応手順
The title compound is prepared by the procedure of Example 2 using 234 g of 3-(tetradecyloxy)benzoic acid methyl ester, 113.0 g of potassium hydroxide, 1 L of methyl alcohol and 120 ml of water. The solid residue is recrystallized from methyl alcohol/ethyl alcohol to give 209 g of the desired product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05208247 |
| 出典データセット | uspto-grants-1993_05 |
| ORD ID | ord-c6728a311c3441738020fdd38caaaa65 |
| 出典メモ | uspto-grants-1993_05 |