HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetonitrile → 1-(Bromomethyl)-3-(tetradecyloxy)benzene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetonitrile | HCID 6342 | — |
| Edukt | Phosphorus tribromide | HCID 24614 | — |
| Edukt | 3-(Tetradecyloxy)benzenemethanol | HCID 10041710 | — |
| Lösungsmittel | Pyridine | HCID 1049 | — |
| Produkt | 1-(Bromomethyl)-3-(tetradecyloxy)benzene | HCID 9977250 | — |
Reaktionsschritte
The title compound is prepared by the procedure of Example 20 using 2.5 g of product from Example 24, 10 ml acetonitrile, 0.339 g of pyridine and 2.11 g of phosphorus tribromide. The product, 2.27 g, is obtained as colorless needles.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05208247 |
| Quelldatensatz | uspto-grants-1993_05 |
| ORD ID | ord-782658fe7dae477880e27f2e4a7f4776 |
| Quellennotiz | uspto-grants-1993_05 |