Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethylformamide → 3-(Tetradecyloxy)benzoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethylformamide | HCID 6228 | — |
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 반응물 | 3-(Tetradecyloxy)benzoic acid | HCID 3262311 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 3-(Tetradecyloxy)benzoyl chloride | HCID 19014949 | — |
반응 단계
To a suspension of 5.0 g of product from Example 23, 0.055 g of dimethylformamide and 70 ml of methylene chloride is added 1.96 ml of oxalyl chloride. The reaction is stirred at room temperature for 22 hours and concentrated. The residue is dissolved in diethyl ether, filtered and concentrated to give 5.28 g of the desired product as cream crystals.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05208247 |
| 출처 데이터셋 | uspto-grants-1993_05 |
| ORD ID | ord-d5ae8f63fb2d41969ca56e994ac5fbd1 |
| 출처 메모 | uspto-grants-1993_05 |