HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → 3-Chloro-4-(tetradecyloxy)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 53824641 | HCID 53824641 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Water | HCID 962 | — |
| Product | 3-Chloro-4-(tetradecyloxy)benzoic acid | HCID 19016283 | 90.5% |
Reaction Steps
The title compound is prepared by the procedure of Example 32 using 125.0 g of product from Example 36 in 1 L of methyl alcohol, 60 ml of water, 400 ml of ethyl alcohol and 54.94 g of potassium hydroxide. The residue is recrystallized from chloroform/hexane to give 109 g of the desired product as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05208247 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-489c5a6c27024d3184ff3303cb2331a2 |
| Source note | uspto-grants-1993_05 |