Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium hydride → HCID 19015591, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium hydride | HCID 24758 | — |
| 반응물 | N-(pyridin-2-ylmethyl)acetamide | HCID 5084090 | — |
| 반응물 | 3-Chloro-4-(tetradecyloxy)benzoyl chloride | HCID 19016288 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | HCID 19015591 | HCID 19015591 | — |
반응 단계
The title compound is prepared by the procedure of Example 27 using 1.31 g of product from Example 38, 0.535 g of product from Example 12, 0.171 g of washed 50% sodium hydride and 12 ml of tetrahydrofuran. The residue is purified by column chromatography (silica gel:35% ethyl acetate/hexane) to give 0.067 g of product as a yellow oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05208247 |
| 출처 데이터셋 | uspto-grants-1993_05 |
| ORD ID | ord-06f7eb774aab41ffa18efbadbe7cb69c |
| 출처 메모 | uspto-grants-1993_05 |