HRID247959

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6328

Methyl iodide

CH3I

反应SMILES：CCCCCCCCCCCCCCOc1ccc(C(=O)N(Cc2ccccn2)C(C)=O)cc1OC

HCID10097364

未命名化合物

PRODUCTS

产物

反应SMILES：CCCCCCCCCCCCCCOc1ccc(C(=O)N(Cc2cccc[n+]2C)C(C)=O)cc1OC.[I-]

HCID10100640

未命名化合物

收率 99.3%

PROCEDURE

实验过程

The title compound is prepared by the procedure of Example 28 using 0.322 g of product from Example 49 and 4.6 g of methyl iodide. The residue is recrystallized from methyl alcohol to give 0.411 g of the desired product as yellow crystals.

WORKUP

后处理

customThe residue is recrystallized from methyl alcohol

来源与证据

来源类型: Open Reaction Database
ORD记录: ord-e22bf4d43c6e474c877cf53c13f6d48f
来源数据集: uspto-grants-1993_05
DOI: 10.6084/m9.figshare.5104873.v1
专利号: US05208247
来源说明: uspto-grants-1993_05

反应SMILES

[C:1]([N:4]([CH2:30][C:31]1[CH:36]=[CH:35][CH:34]=[CH:33][N:32]=1)[C:5](=[O:29])[C:6]1[CH:11]=[CH:10][C:9]([O:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26])=[C:8]([O:27][CH3:28])[CH:7]=1)(=[O:3])[CH3:2].[CH3:37][I:38]>>[I-:38].[C:1]([N:4]([CH2:30][C:31]1[CH:36]=[CH:35][CH:34]=[CH:33][N+:32]=1[CH3:37])[C:5](=[O:29])[C:6]1[CH:11]=[CH:10][C:9]([O:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26])=[C:8]([O:27][CH3:28])[CH:7]=1)(=[O:3])[CH3:2]