HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → p-Tetradecyloxyphenylacetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | [4-(Tetradecyloxy)phenyl]acetic acid methyl ester | HCID 10316608 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | p-Tetradecyloxyphenylacetic acid | HCID 10472964 | 84.1% |
Reaction Steps
The title compound is prepared by the procedure of Example 32 using 75 g of product from Example 51, 34.8 g of potassium hydroxide, 45 ml of water and 800 ml of ethyl alcohol. The residue is recrystallized from carbon tetrachloride/hexane to give 60.6 g of the desired product as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05208247 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-5b5faf5a834a4acba131ff2cbd95162f |
| Source note | uspto-grants-1993_05 |